CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE

Base Information

• Chemical Name: CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE
• CAS No.: 29118-71-6
• Molecular Formula: C₁₂H₁₉ClN₂O
• Molecular Weight: 242.749
• Hs Code.: 2928000090
• Mol file: 29118-71-6.mol

Synonyms:CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE;

Chemical Property of CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 41.46000
• Density: 1.25g/cm³
• LogP: 2.93450

Purity/Quality:

99% ^*data from raw suppliers

CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE

There total 2 articles about CHLORO-ACETIC ACID (1,7,7-TRIMETHYL-BICYCLO[2.2.1]HEPT-2-YLIDENE)-HYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one (736109-58-3,787517-91-3,68546-28-1) + chloroacetic acid ethyl ester (105-39-5) → Chloro-acetic acid [1,7,7-trimethyl-bicyclo[2.2.1]hept-(2Z)-ylidene]-hydrazide (29118-71-6)

Guidance literature:

Multistep reaction; (i) N₂H₄*H₂O, (ii) /BRN= 1907611/;

DOI:10.1246/bcsj.43.2257

Reference yield:

→ Chloro-acetic acid [1,7,7-trimethyl-bicyclo[2.2.1]hept-(2E)-ylidene]-hydrazide (29118-71-6)

Guidance literature:

Chloracetylhydrazin, d-Campher;

DOI:10.1246/bcsj.43.2257

upstream raw materials:

1,7,7-trimethyl-bicyclo[2.2.1]heptan-2-one

chloroacetic acid ethyl ester

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