C₄₀H₅₉NO₄Si

Base Information

Chemical Name:C₄₀H₅₉NO₄Si
CAS No.:1404379-97-0
Molecular Formula:C₄₀H₅₉NO₄Si
Molecular Weight:645.998
Hs Code.:

C<sub>40</sub>H<sub>59</sub>NO<sub>4</sub>Si

Synonyms:

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Chemical Property of C₄₀H₅₉NO₄Si

Chemical Property:

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Technology Process of C₄₀H₅₉NO₄Si

There total 22 articles about C₄₀H₅₉NO₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 646-07-1
4-Methylpentanoic acid

: 1404379-97-0
C₄₀H₅₉NO₄Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

2.1: 1,1,3,3-Tetramethyldisiloxane / (Ph₃P)2IrCl(CO) / toluene / 2 h / 20 °C

3.1: hydroquinone / acetonitrile / 95 °C

4.1: methyl p-toluene sulfonate / water / 2 h / 110 °C

4.2: 4 h / 95 °C

5.1: hydrogen / rhodium contaminated with carbon / tetrahydrofuran / 7 h / 20 °C / 760.05 Torr

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 20 °C

7.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C

7.2: Cooling with ice

8.1: triphenylphosphine / dichloromethane / 0.33 h / Cooling with ice

8.2: 0.33 h / Cooling with ice

9.1: n-butyllithium / tetrahydrofuran

10.1: 1H-imidazole / N,N-dimethyl-formamide

11.1: pyridine / methanol

With pyridine; 1H-imidazole; n-butyllithium; 1,1,3,3-Tetramethyldisiloxane; hydrogen; diisobutylaluminium hydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; hydroquinone; methyl p-toluene sulfonate; triphenylphosphine; rhodium contaminated with carbon; (Ph₃P)2IrCl(CO); In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;

Reference yield:

: 96556-40-0
methyl-3-(benzyloxy)-2.2-dimethylpropionate

: 1404379-97-0
C₄₀H₅₉NO₄Si

Guidance literature:: Multi-step reaction with 12 steps

1: lithium borohydride / tetrahydrofuran

2: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

3: toluene

4: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

5: sodium hydroxide / ethanol

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

7: tetrahydrofuran

8: palladium on activated charcoal / tetrahydrofuran

9: potassium tert-butylate / toluene

10: n-butyllithium / tetrahydrofuran

11: 1H-imidazole / N,N-dimethyl-formamide

12: pyridine / methanol

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 14002-80-3
Methyl 2,2-dimethyl-3-hydroxypropionate

: 1404379-97-0
C₄₀H₅₉NO₄Si

Guidance literature:: Multi-step reaction with 13 steps

1: diethyl ether

2: lithium borohydride / tetrahydrofuran

3: triethylamine; pyridine-SO₃ complex / dichloromethane; dimethyl sulfoxide

4: toluene

5: sodium tetrahydroborate; methanol / cobalt(II) chloride hexahydrate / N,N-dimethyl-formamide

6: sodium hydroxide / ethanol

7: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / chloroform

8: tetrahydrofuran

9: palladium on activated charcoal / tetrahydrofuran

10: potassium tert-butylate / toluene

11: n-butyllithium / tetrahydrofuran

12: 1H-imidazole / N,N-dimethyl-formamide

13: pyridine / methanol

With pyridine; 1H-imidazole; methanol; dmap; sodium tetrahydroborate; lithium borohydride; n-butyllithium; pyridine-SO₃ complex; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; cobalt(II) chloride hexahydrate; palladium on activated charcoal; potassium tert-butylate; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;