C₂₈H₃₁Cl₂N₃O₄S

Base Information

• Chemical Name: C₂₈H₃₁Cl₂N₃O₄S
• CAS No.: 1401533-14-9
• Molecular Formula: C₂₈H₃₁Cl₂N₃O₄S
• Molecular Weight: 576.544

Synonyms:

Chemical Property of C₂₈H₃₁Cl₂N₃O₄S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₃₁Cl₂N₃O₄S

There total 6 articles about C₂₈H₃₁Cl₂N₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,4-Dichlor-benzo--thiophen-2-carbonsaeurechlorid (34576-86-8) + C19H29N3O3 (1401533-28-5) → C28H31Cl2N3O4S (1401533-14-9)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.bmc.2012.08.026

Reference yield:

4-aminopiperidine (13035-19-3) → C28H31Cl2N3O4S (1401533-14-9)

Guidance literature:

Multi-step reaction with 5 steps

1: toluene / 5.5 h / Inert atmosphere; Reflux

2: toluene / 14.08 h / 0 - 20 °C / Inert atmosphere

3: potassium hydrogensulfate; water / tert-butyl methyl ether / 4 h / 20 °C / Inert atmosphere

4: magnesium sulfate; sodium tetrahydroborate / ethanol / 22 h / 20 - 70 °C / Inert atmosphere

5: dmap; triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; potassium hydrogensulfate; water; magnesium sulfate; triethylamine; In ethanol; dichloromethane; tert-butyl methyl ether; toluene;

DOI:10.1016/j.bmc.2012.08.026

Reference yield:

N-phenylmethylidenepiperidinyl-4-amine (1029643-92-2) → C28H31Cl2N3O4S (1401533-14-9)

Guidance literature:

Multi-step reaction with 4 steps

1: toluene / 14.08 h / 0 - 20 °C / Inert atmosphere

2: potassium hydrogensulfate; water / tert-butyl methyl ether / 4 h / 20 °C / Inert atmosphere

3: magnesium sulfate; sodium tetrahydroborate / ethanol / 22 h / 20 - 70 °C / Inert atmosphere

4: dmap; triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

With dmap; sodium tetrahydroborate; potassium hydrogensulfate; water; magnesium sulfate; triethylamine; In ethanol; dichloromethane; tert-butyl methyl ether; toluene;

DOI:10.1016/j.bmc.2012.08.026

upstream raw materials:

4-aminopiperidine

N-phenylmethylidenepiperidinyl-4-amine

4-(benzylidene-amino)-piperidine-1-carboxylic acid tert-butyl ester

1-(tert-butoxycarbonyl)-4-aminopiperidine

Downstream raw materials:

C₂₃H₂₃Cl₂N₃O₂S

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1401533-14-9 C₂₈H₃₁Cl₂N₃O₄S

Send

Send

Metric Ton KG G Pound L ML

Send

Send