3-chloroanilinium bromide

Base Information

• Chemical Name: 3-chloroanilinium bromide
• CAS No.: 33670-60-9
• Molecular Formula: Br*C₆H₇ClN
• Molecular Weight: 208.485
• Mol file: 33670-60-9.mol

Synonyms:

Chemical Property of 3-chloroanilinium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-chloroanilinium bromide

There total 6 articles about 3-chloroanilinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-chloro-aniline (108-42-9) → 3-chloroanilinium bromide (33670-60-9)

Guidance literature:

With hydrogen bromide; In ethanol;

DOI:10.1021/cg201683p

Reference yield:

m-chlorobenzoyl bromide (34549-54-7) + 3-chloro-aniline (108-42-9) → 3-Chloro-N-(3-chlorophenyl)benzamide (10286-92-7) + 3-chloroanilinium bromide (33670-60-9)

Guidance literature:

In benzene; at 10 ℃; Rate constant; Thermodynamic data; oth. temperature, E(activ.), ΔH(activ.), ΔS'(activ.);

Reference yield:

m-nitrobenzoyl bromide (13277-62-8) + 3-chloro-aniline (108-42-9) → 3-Nitro-benzoesaeure-<3-chlor-anilid> (2585-22-0) + 3-chloroanilinium bromide (33670-60-9)

Guidance literature:

In benzene; at 10 ℃; Rate constant; Thermodynamic data; oth. temperature, E(activ.), ΔH(activ.), ΔS'(activ.);

upstream raw materials:

Benzoyl bromide

3-chloro-aniline

m-chlorobenzoyl bromide

m-nitrobenzoyl bromide

Downstream raw materials:

bis(3-chloroaniline) cobalt(II) bromide

Refernces

• 1、 Shpan'ko, I. V.,Goncharov, A. N.,Likhomanenko, E. E.. "JOINT EFFECT OF STRUCTURE OF REAGENTS AND TEMPERATURE ON REACTIVITY OF AROYL BROMIDE-PRIMARY ARYLAMINE SYSTEMS IN BENZENE. CROSSED CORRELATION". . p. 522 - 530. Retrieved 2007/10/02.