PhC(O)N(Pr(i))Zn(Bu(t))2Li*2thf

Base Information

Chemical Name:PhC(O)N(Pr(i))Zn(Bu(t))2Li*2thf
CAS No.:585534-99-2
Molecular Formula:C₅₂H₉₂Li₂N₂O₆Zn₂
Molecular Weight:985.974
Hs Code.:

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Chemical Property of PhC(O)N(Pr(i))Zn(Bu(t))2Li*2thf

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Technology Process of PhC(O)N(Pr(i))Zn(Bu(t))2Li*2thf

There total 1 articles about PhC(O)N(Pr(i))Zn(Bu(t))2Li*2thf which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 5440-69-7
N-isopropylbenzamide

: 544-97-8
dimethyl zinc(II)

: 594-19-4
tert.-butyl lithium

: 585534-99-2
PhC(O)N(Pr(i))Zn(Bu(t))2Li*2thf

Guidance literature:: In tetrahydrofuran; toluene; pentane; under N2 atm. N-methyl benzamide in toluene was treated with ZnMe2 in toluene, react. mixt. was cooled to -78°C, t-BuLi in pentane was added, react. mixt. was allowed to warm to room temp., THF was added; soln. was concd. and stored at -30°C for 2 days; elem. anal.;
DOI:10.1039/b210479b