Borinic acid, dicyclohexyl-, (1Z)-1-ethyl-1-butenyl ester

Base Information

Chemical Name:Borinic acid, dicyclohexyl-, (1Z)-1-ethyl-1-butenyl ester
CAS No.:134435-90-8
Molecular Formula:C₁₈H₃₃BO
Molecular Weight:276.27
Hs Code.:

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Chemical Property of Borinic acid, dicyclohexyl-, (1Z)-1-ethyl-1-butenyl ester

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Technology Process of Borinic acid, dicyclohexyl-, (1Z)-1-ethyl-1-butenyl ester

There total 1 articles about Borinic acid, dicyclohexyl-, (1Z)-1-ethyl-1-butenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50396-96-8,130981-55-4,2497-21-4,50396-87-7
E-4-hexen-3-one

: 1568-65-6
bis(cyclohexanyl)borane

: 134435-90-8
(C₆H₁₁)2(OC(Et)CHCH₂Me)borane

Guidance literature:: In chloroform; dropwise addn. of the unsaturated ketone to the borane in THF over 10 min at room temp.;
DOI:10.1039/c39900001680

Reference yield: 57.0%

: 134435-90-8
(C₆H₁₁)2(OC(Et)CHCH₂Me)borane

: 100-52-7
benzaldehyde

: 132455-66-4
syn-4-(phenylhydroxymethyl)-3-hexanone

Guidance literature:: With water; In chloroform; treating the soln. of the B compd. in THF at 20°C with the aldehyde, stirring for 4 h at the same temp., quenching with water and stirring for 30 min; column-chromy. on silica gel;
DOI:10.1039/c39900001680