Technology Process of C11H14FN
There total 7 articles about C11H14FN which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: copper(l) iodide / tetrahydrofuran; 2-methyltetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3: hydrazine / toluene / 90 °C / Inert atmosphere
4: dichloromethane / Inert atmosphere
5: chiralpak AD-H / methanol; carbon dioxide / Inert atmosphere
6: hydrogenchloride / Inert atmosphere
With
hydrogenchloride; copper(l) iodide; di-isopropyl azodicarboxylate; triphenylphosphine; hydrazine;
In
tetrahydrofuran; 2-methyltetrahydrofuran; methanol; dichloromethane; carbon dioxide; toluene;
DOI:10.1021/jm201019k
- Guidance literature:
-
Multi-step reaction with 2 steps
1: chiralpak AD-H / methanol; carbon dioxide / Inert atmosphere
2: hydrogenchloride / Inert atmosphere
With
hydrogenchloride;
In
methanol; carbon dioxide;
DOI:10.1021/jm201019k
- Guidance literature:
-
Multi-step reaction with 6 steps
1: copper(l) iodide / tetrahydrofuran; 2-methyltetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3: hydrazine / toluene / 90 °C / Inert atmosphere
4: dichloromethane / Inert atmosphere
5: chiralpak AD-H / methanol; carbon dioxide / Inert atmosphere
6: hydrogenchloride / Inert atmosphere
With
hydrogenchloride; copper(l) iodide; di-isopropyl azodicarboxylate; triphenylphosphine; hydrazine;
In
tetrahydrofuran; 2-methyltetrahydrofuran; methanol; dichloromethane; carbon dioxide; toluene;
DOI:10.1021/jm201019k