ethyl (E)-5-phenylpent-3-enoate-2,4-d₂

Base Information

• Chemical Name: ethyl (E)-5-phenylpent-3-enoate-2,4-d₂
• CAS No.: 1646185-11-6
• Molecular Formula: C₁₃H₁₆O₂
• Molecular Weight: 206.253
• Mol file: 1646185-11-6.mol

Synonyms:

Chemical Property of ethyl (E)-5-phenylpent-3-enoate-2,4-d₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of ethyl (E)-5-phenylpent-3-enoate-2,4-d₂

There total 1 articles about ethyl (E)-5-phenylpent-3-enoate-2,4-d₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

penta-3,4-dienoic acid ethyl ester (30332-99-1) + phenylmagnesium bromide (100-58-3) → ethyl (E)-5-phenylpent-3-enoate-2,4-d2 (1646185-11-6)

Guidance literature:

penta-3,4-dienoic acid ethyl ester; With n-butyllithium; diisopropylamine; In diethyl ether; hexane; for 0.5h;

phenylmagnesium bromide; With copper(l) iodide; In diethyl ether; hexane; at -78 - -20 ℃; for 3h; Inert atmosphere;

With deuteroacetic acid; hydrogen chloride; In diethyl ether; hexane; water-d2; at 20 ℃; stereoselective reaction;

DOI:10.1002/chem.201403294

upstream raw materials:

penta-3,4-dienoic acid ethyl ester

phenylmagnesium bromide