(3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

Base Information

Chemical Name:(3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one
CAS No.:1365541-61-2
Molecular Formula:C₃₄H₅₃NO₄Si₂
Molecular Weight:595.97
Hs Code.:

(3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

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Chemical Property of (3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

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Technology Process of (3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

There total 1 articles about (3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1365541-51-0
methyl ((S)-1-(2-(2-((3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-2-oxopyrrolidin-3-yl)ethyl)-2-(4-bromobenzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-yl)carbamate

: 1365541-61-2
(3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

: 1365541-59-8
methyl ((S)-1-(2-(2-((3R,4R)-3-benzyl-4-hydroxy-1-((1S,2R)-2-hydroxy-2,3-dihydro-1H-inden-1-yl)-2-oxopyrrolidin-3-yl)ethyl)-2-(4-bromobenzyl)hydrazinyl)-3,3-dimethyl-1-oxobutan-2-yl)carbamate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/jm201620t

Reference yield:

: 1365541-61-2
(3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

: C₃₄H₅₁NO₄Si₂

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm201620t

Reference yield:

: 1365541-61-2
(3R,4R)-3-benzyl-4-((tert-butyldimethylsilyl)oxy)-1-((1S,2R)-2-((tert-butyldimethylsilyl)oxy)-2,3-dihydro-1H-inden-1-yl)-3-(2-hydroxyethyl)pyrrolidin-2-one

: C₅₄H₇₇N₅O₆Si₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

2.1: acetic acid / tetrahydrofuran / 20 °C

2.2: 20 °C

With Dess-Martin periodane; acetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm201620t