C₂₂H₁₉FN₄O₃

Base Information

Chemical Name:C₂₂H₁₉FN₄O₃
CAS No.:1372132-40-5
Molecular Formula:C₂₂H₁₉FN₄O₃
Molecular Weight:406.416
Hs Code.:

C<sub>22</sub>H<sub>19</sub>FN<sub>4</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₁₉FN₄O₃

Chemical Property:

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Technology Process of C₂₂H₁₉FN₄O₃

There total 7 articles about C₂₂H₁₉FN₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1300031-61-1
[3-(3,5-dimethyl-4-isoxazolyl)-4-(methyloxy)phenyl]amine

: 1372132-40-5
C₂₂H₁₉FN₄O₃

Guidance literature:: Multi-step reaction with 6 steps

1: 1 h / 130 °C

2: diphenylether / 0.75 h / 255 °C

3: sodium hydroxide / ethanol / Reflux

4: trichlorophosphate / 4 h / Heating

5: ammonium hydroxide / tetrahydrofuran / 0.5 h / Cooling with ice

6: Heating

With ammonium hydroxide; diphenylether; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2012.01.125

Reference yield:

: C₁₆H₁₂Cl₂N₂O₃

: 1372132-40-5
C₂₂H₁₉FN₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / tetrahydrofuran / 0.5 h / Cooling with ice

2: Heating

With ammonium hydroxide; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2012.01.125

Reference yield:

: 16114-47-9
3,5-dimethylisoxazole-4-boronic acid

: 1372132-40-5
C₂₂H₁₉FN₄O₃

Guidance literature:: Multi-step reaction with 8 steps

1: caesium carbonate / 1,2-dimethoxyethane; water / 4 h / 90 °C / Inert atmosphere

2: palladium on activated charcoal; hydrogen; sodium sulfite / ethanol; ethyl acetate / 24 h

3: 1 h / 130 °C

4: diphenylether / 0.75 h / 255 °C

5: sodium hydroxide / ethanol / Reflux

6: trichlorophosphate / 4 h / Heating

7: ammonium hydroxide / tetrahydrofuran / 0.5 h / Cooling with ice

8: Heating

With ammonium hydroxide; diphenylether; palladium on activated charcoal; hydrogen; caesium carbonate; sodium hydroxide; sodium sulfite; trichlorophosphate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; water; ethyl acetate; 1: Suzuki coupling;
DOI:10.1016/j.bmcl.2012.01.125