(1S,2R,3S)-2-Fluoro-3-trityloxymethyl-cyclopentylamine

Base Information

Chemical Name:(1S,2R,3S)-2-Fluoro-3-trityloxymethyl-cyclopentylamine
CAS No.:129746-07-2
Molecular Formula:C₂₅H₂₆FNO
Molecular Weight:375.486
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2R,3S)-2-Fluoro-3-trityloxymethyl-cyclopentylamine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
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MSDS Files:: SDS file from LookChem

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Technology Process of (1S,2R,3S)-2-Fluoro-3-trityloxymethyl-cyclopentylamine

There total 13 articles about (1S,2R,3S)-2-Fluoro-3-trityloxymethyl-cyclopentylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: C₂₅H₂₄FN₃O

: 129746-07-2,129829-84-1,137767-70-5
(1S,2R,3S)-2-Fluoro-3-trityloxymethyl-cyclopentylamine

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethanol;
DOI:10.1039/c39900000151

Reference yield: 99.0%

: (1β,2α,3β)-1-azido-2-fluoro-3-triphenylmethyloxymethylcyclopentane

: 129746-07-2,129829-84-1,137767-70-5
(1β,2α,3β)-2-fluoro-3-triphenylmethoxymethylcyclopentylamine

Guidance literature:: With hydrogen; Lindlar's catalyst; In ethanol; for 3h; under 760 Torr; Ambient temperature;

Reference yield:

: 119895-90-8
triphenylmethoxymethylcyclopent-2-ene

: 129746-07-2,129829-84-1,137767-70-5
(1β,2α,3β)-2-fluoro-3-triphenylmethoxymethylcyclopentylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 1) dibromodimethylhydantoin, 2) potassium carbonate / 1) acetone, water, 0 deg C, 2) methanol, room temperature, overnight

2: 84 percent / sodium azide, ammonium chloride / aq. ethanol / 72 h / 100 °C

3: 21 percent / diethylaminosulphur trifluoride / CH₂Cl₂ / 0.17 h / 0 °C

4: 99 percent / H₂ / Lindlar / ethanol / 3 h / 760 Torr / Ambient temperature

With sodium azide; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; diethylamino-sulfur trifluoride; ammonium chloride; hydrogen; potassium carbonate; Lindlar's catalyst; In ethanol; dichloromethane;