2-menthoxyethanethiol

Base Information

Chemical Name:2-menthoxyethanethiol
CAS No.:118617-60-0
Molecular Formula:C₁₂H₂₄OS
Molecular Weight:216.388
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-menthoxyethanethiol

Chemical Property:

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Technology Process of 2-menthoxyethanethiol

There total 2 articles about 2-menthoxyethanethiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2216-51-5
(-)-menthol

: 118617-60-0
2-menthoxyethanethiol

Guidance literature:: Multi-step reaction with 2 steps

1: Hg(OAc)2

2: 1.) benzoyl peroxide 2.) 20percent aq. NaOH / 1.) RT, 1 h 2.) MeOH, reflux, 1 h; var. of step 2.): LiAlH₄, ether, 2 h, reflux

With sodium hydroxide; Perbenzoic acid; mercury(II) diacetate;
DOI:10.1016/S0040-4020(01)87684-5

Reference yield:

: 5989-48-0,7637-09-4,7637-10-7,7637-11-8,23960-73-8,46173-76-6,127642-93-7,3885-03-8
(1S,2R,4R)-1-isopropyl-4-methyl-(2-vinyloxy)cyclohexane

: 68-11-1
mercaptoacetic acid

: 118617-60-0
2-menthoxyethanethiol

Guidance literature:: With sodium hydroxide; Perbenzoic acid; Yield given. Multistep reaction; 1.) RT, 1 h 2.) MeOH, reflux, 1 h; var. of step 2.): LiAlH₄, ether, 2 h, reflux;
DOI:10.1016/S0040-4020(01)87684-5

Reference yield:

: 118617-60-0
2-menthoxyethanethiol

: 112052-04-7,112136-67-1
trans-4-(2-methoxyethylsulfonyl)-5-methyl-5-phenyl-2-oxazoline

Guidance literature:: Multi-step reaction with 4 steps

2: 85percent m-CPBA

3: 65 percent / POCl₃, Et₃N / 0.5 h / 0 °C

4: 74 percent / benzyltriethylammonium chloride, 50percent aq. NaOH / benzene / 3 h / 10 - 15 °C

With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In benzene;
DOI:10.1016/S0040-4020(01)87684-5