Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)-

Base Information

Chemical Name:Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)-
CAS No.:134786-08-6
Molecular Formula:C11H21N
Molecular Weight:167.294
Hs Code.:
DSSTox Substance ID:DTXSID10441667
Nikkaji Number:J1.103.191I
Wikidata:Q82258535
Mol file:134786-08-6.mol

Synonyms:134786-08-6;Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)-;1-(2-methylprop-2-enyl)cyclohexane-methylamine;SCHEMBL19601685;DTXSID10441667;1-(2-Methyl-2-propenyl)cyclohexanemethanamine

Suppliers and Price of Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)-

Chemical Property:

XLogP3:3.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:167.167399674
Heavy Atom Count:12
Complexity:154

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=C)CC1(CCCCC1)CN

Technology Process of Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)-

There total 6 articles about Cyclohexanemethanamine, 1-(2-methyl-2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 134786-04-2
1-(2-Methyl-allyl)-cyclohexanecarboxylic acid amide

: 134786-08-6
1-(2-methylprop-2-enyl)cyclohexane-methylamine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 2.5h; Heating;
DOI:10.1016/S0040-4020(01)96036-3

Reference yield:

: 766-05-2
cyclohexane carbonitrile

: 134786-08-6
1-(2-methylprop-2-enyl)cyclohexane-methylamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: LDA / tetrahydrofuran / -78 °C

1.2: 70 percent / tetrahydrofuran / 20 °C

2.1: 83 percent / LiAlH₄ / diethyl ether / 20 °C

With lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja043278q

Reference yield:

: 4630-82-4
methyl cyclohexylcarboxylate

: 134786-08-6
1-(2-methylprop-2-enyl)cyclohexane-methylamine

Guidance literature:: Multi-step reaction with 5 steps

1: iPr₂NLi / tetrahydrofuran / -78 °C

2: 15percent ethanolic KOH / Heating

3: sodium, oxalyl chloride / diethyl ether / Heating

4: ammonia / diethyl ether / ice-cooling

5: 92 percent / LiAlH₄ / tetrahydrofuran / 2.5 h / Heating

With potassium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; ammonia; sodium; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(01)96036-3