trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate

Base Information

Chemical Name:trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate
CAS No.:835890-05-6
Molecular Formula:BF₄*C₅₆H₄₈IrO₂P₂
Molecular Weight:1093.97
Hs Code.:

trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate

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Technology Process of trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate

There total 1 articles about trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 835890-35-2
trans-[IrH(PPh₃)2(C(C₆H₅)=CHC(CH₃)O)(acetone)]BF₄

: 1817-57-8
4-phenyl-3-butyne-2-one

: 835890-05-6
trans-bis(triphenylphosphine)(η2-(O,C1)-1-phenylbut-1-en-3-on-1-yl)(η2-(O,C2)-1-phenylbut-1-(E)-en-3-one-2-yl)iridium(III) tetrafluoroborate

Guidance literature:: In dichloromethane; (Ar); alkyne (2 equiv.) was added to stirred soln. of Ir complex in CH2Cl2; soln. was refluxed for 5 h; concd.; Et2O added; recrystd. (CH2Cl2/Et2O); elem. anal.;
DOI:10.1021/om049271z