TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz

Base Information

Chemical Name:TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz
CAS No.:860776-07-4
Molecular Formula:C₃₃H₄₈N₂Ti
Molecular Weight:520.638
Hs Code.:

TiCp*[1,2-C<sub>6</sub>H<sub>4</sub>(NCH<sub>2</sub>(t)Bu)2]Bz

Synonyms:

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Chemical Property of TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz

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Technology Process of TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz

There total 1 articles about TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 830323-31-4
(η5-pentamethylcyclopentadienyl)(N,N'-bis(neopentyl)-1,2-phenylenediamido)chlorotitanium

: 6921-34-2
benzylmagnesium chloride

: 860776-07-4
TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz

Guidance literature:: In tetrahydrofuran; hexane; Ar, a soln. of Mg compd. (THF) added to a soln. of Ti compd. (hexane) at-78°C, stirred for 12 h, warmed to room temp.; filtered, cooled to -40°C, ppt. filtered, recrystd. (pentane); elem. anal.;
DOI:10.1002/ejic.200400661

Reference yield:

: 860776-07-4
TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz

: 1109-15-5
tris(pentafluorophenyl)borate

: TiCp*[1,2-C6H4(NCH2(t)Bu)2][μ-CH2PhB(C6F5)3]

Guidance literature:: In benzene-d6; under Ar; C6D6 was added to a mixt. of Ti-contg. compd. and B(C6F5)3; NMR spectra studies;
DOI:10.1021/om051088y

Reference yield:

: 1665-00-5
dichloromethane-d2

: 860776-07-4
TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2]Bz

: 1109-15-5
tris(pentafluorophenyl)borate

: (TiCp*[1,2-C₆H₄(NCH₂(t)Bu)2](CD₂Cl₂)n)[PhCH₂B(C₆F₅)3]

Guidance literature:: In benzene-d6; in the drybox; C6D6 was added to a mixt. of Ti-contg. compd. (0.019 mmol) and B(C6F5)3 (0.019 mmol) in a Young tube; after 10 h the solvent was removed by decantation, the residue was dried in vac., and CD2Cl2 was added; NMR spectra studies;
DOI:10.1021/om051088y