Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester

Base Information

Chemical Name:Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester
CAS No.:118190-44-6
Molecular Formula:C₂₀H₂₅NO₉
Molecular Weight:423.42
Hs Code.:

Synonyms:

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Chemical Property of Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester

Chemical Property:

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Technology Process of Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester

There total 14 articles about Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118190-40-2
Benzoic acid (2S,3S,4R,5R,6S)-5-benzyloxycarbonylamino-2-bromomethyl-4-hydroxy-6-methoxy-tetrahydro-pyran-3-yl ester

: 118190-44-6,118244-79-4
Acetic acid (1R,2R,3S,4R,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) DMAP; 2.) silver fluoride / 1.)CH₂Cl₂; 2.) pyridine

2: 71 percent / mercuric chloride / acetone; H₂O / Heating

3: H(+) / CH₂Cl₂

4: zinc borohydride / tetrahydrofuran

6: 1.) ruthenium tetroxide; 2.) zinc borohydride / 1.) CH₂Cl₂, CCl₄; 2.) CH₂Cl₂

With dmap; ruthenium tetroxide; zinc borohydride; silver fluoride; hydrogen cation; mercury dichloride; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1246/cl.1988.1235

Reference yield:

: 118190-40-2
Benzoic acid (2S,3S,4R,5R,6S)-5-benzyloxycarbonylamino-2-bromomethyl-4-hydroxy-6-methoxy-tetrahydro-pyran-3-yl ester

: 118190-44-6,118244-79-4
Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) DMAP; 2.) silver fluoride / 1.)CH₂Cl₂; 2.) pyridine

2: 71 percent / mercuric chloride / acetone; H₂O / Heating

3: H(+) / CH₂Cl₂

4: zinc borohydride / tetrahydrofuran

With dmap; zinc borohydride; silver fluoride; hydrogen cation; mercury dichloride; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1246/cl.1988.1235

Reference yield:

: 118190-41-3
C₂₉H₂₇NO₈

: 118190-44-6,118244-79-4
Acetic acid (1R,2R,3S,4S,6S)-2,6-diacetoxy-3-benzyloxycarbonylamino-4-hydroxy-cyclohexyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 71 percent / mercuric chloride / acetone; H₂O / Heating

2: H(+) / CH₂Cl₂

3: zinc borohydride / tetrahydrofuran

With zinc borohydride; hydrogen cation; mercury dichloride; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1246/cl.1988.1235