Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid

Base Information

• Chemical Name: Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid
• CAS No.: 103929-44-8
• Molecular Formula: C₁₆H₁₆ClN₃O
• Molecular Weight: 301.776
• Mol file: 103929-44-8.mol

Synonyms:

Chemical Property of Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid

There total 2 articles about Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

benzoyl chloride (98-88-4) + 2-Amino-2-(4-chlorphenylazo)-propan → Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid (103929-44-8)

Guidance literature:

In pyridine; benzene; at 20 ℃; for 6h;

DOI:10.1007/BF00811104

Reference yield:

Acetone (4-Chlorophenyl)hydrazone (1200-11-9) → Benzoesaeure-N-<1-(4-chlorphenylazo)-1-methylethyl>-amid (103929-44-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Br₂/AcNH₂; 2.) a) liquid NH₃, b) 10percent K₂CO₃ / 1.) CH₂Cl₂, 15 min, 0 degC; 2.) 90 min

2: 48 percent / pyridine; benzene / 6 h / 20 °C

With acetamide; ammonia; bromine; potassium carbonate; In pyridine; benzene;

DOI:10.1007/BF00811104

upstream raw materials:

benzoyl chloride

Acetone (4-Chlorophenyl)hydrazone