4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

Base Information

Chemical Name:4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin
CAS No.:75837-00-2
Molecular Formula:C₃₃H₂₈N₄O₁₀
Molecular Weight:640.606
Hs Code.:

4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

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Chemical Property of 4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

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Technology Process of 4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

There total 2 articles about 4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 103-71-9
phenyl isocyanate

: 75836-98-5
8-(α-Hydroxy-2-nitrobenzyl)-4-methoxy-6-methyl-10-(2-nitrophenyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

: 75837-00-2
4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

Guidance literature:: In chloroform; 1.) 50 deg C, 2 h, 2.) overnight;
DOI:10.1002/ardp.19803130811

Reference yield:

: 82-54-2
4-methoxy-6-methyl-5,6,7,8-tetrahydro-1,3-dioxolo[4,5-g]isoquinolin-5-ol

: 75837-00-2
4-Methoxy-6-methyl-10-(2-nitrophenyl)-8-(2-nitro-α-phenyl-carbamoyloxy-benzyl)-5,6,7,8-tetrahydro-5,7-(epoxymethano)-1,3-dioxolo<4,5-g>isochinolin

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / ethanol / 0.67 h / Heating

2: 41 percent / CHCl₃ / 1.) 50 deg C, 2 h, 2.) overnight

In ethanol; chloroform;
DOI:10.1002/ardp.19803130811