5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one

Base Information

Chemical Name:5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one
CAS No.:51066-28-5
Molecular Formula:C₂₄H₁₉NO
Molecular Weight:337.421
Hs Code.:

5-benzyl-11,12-dihydrobenzo<c>phenanthridin-6(5H)-one

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Chemical Property of 5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one

Chemical Property:

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Technology Process of 5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one

There total 4 articles about 5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 124985-32-6
N-benzyl-N-(1,2-dihydronaphth-4-yl)-2-iodobenzamide

: 51066-28-5
5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one

: 129574-22-7
C₂₄H₂₁NO

Guidance literature:: With triethyl borane; tri-n-butyl-tin hydride; In hexane; toluene; at 20 ℃; for 4h;

Reference yield:

: 32851-51-7
N-(3,4-dihydronaphthalen-1(2H)-ylidene)-1-phenylmethanamine

: 51066-28-5
5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / triethylamine / 1,2-dimethoxy-ethane / 1.) -60 deg C, 1 h, 2.) up to r.t., 3.) r.t., 2 h

2: 1.) isoamyl nitrite, trichloroacetic acid / multistep reaction: 1. DME, a) 0 deg C, 15 min, b) r.t., 90 min, 2.) DME, reflux; other pyrrolinediones

With triethylamine; isopentyl nitrite; trichloroacetic acid; In 1,2-dimethoxyethane;
DOI:10.1021/jo00048a024

Reference yield:

: 100-46-9
benzylamine

: 51066-28-5
5-benzyl-11,12-dihydrobenzophenanthridin-6(5H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / p-toluenesulfonic acid / toluene / 12 h / Heating

2: 74 percent / triethylamine / 1,2-dimethoxy-ethane / 1.) -60 deg C, 1 h, 2.) up to r.t., 3.) r.t., 2 h

3: 1.) isoamyl nitrite, trichloroacetic acid / multistep reaction: 1. DME, a) 0 deg C, 15 min, b) r.t., 90 min, 2.) DME, reflux; other pyrrolinediones

With toluene-4-sulfonic acid; triethylamine; isopentyl nitrite; trichloroacetic acid; In 1,2-dimethoxyethane; toluene;
DOI:10.1021/jo00048a024