Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

Base Information

Chemical Name:Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside
CAS No.:51996-42-0
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:
DSSTox Substance ID:DTXSID401179307
Nikkaji Number:J530.361C

Synonyms:51996-42-0;DTXSID401179307;Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

Suppliers and Price of Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:265.13140809
Heavy Atom Count:19
Complexity:304

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1C(C(CC(O1)OC)NC(=O)C2=CC=CC=C2)O
Isomeric SMILES:C[C@H]1[C@H]([C@H](C[C@@H](O1)OC)NC(=O)C2=CC=CC=C2)O

Technology Process of Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside

There total 12 articles about Methyl 3-(benzoylamino)-2,3,6-trideoxy-alpha-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 97327-52-1,116429-78-8
methyl 3-benzamido-4-O-benzoyl-2-bromo-2,3,6-trideoxy-α-DL-galactopyranoside

: 17016-64-7,51869-36-4,51996-42-0,54656-60-9,57918-57-7,58769-79-2,62812-43-5,64429-66-9,67776-32-3,80483-26-7,97372-44-6
methyl 3-benzamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 0.5h; Ambient temperature;

Reference yield: 94.0%

: 62774-42-9,67758-45-6,92206-23-0,97327-53-2,116429-79-9
methyl 3-benzamido-4-O-benzoyl-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside

: 17016-64-7,51869-36-4,51996-42-0,54656-60-9,57918-57-7,58769-79-2,62812-43-5,64429-66-9,67776-32-3,80483-26-7,97372-44-6
methyl 3-benzamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside

Guidance literature:: With sodium; In methanol; for 1h; Ambient temperature;

Reference yield:

: 614-28-8
N-benzoylbenzamide

: 17016-64-7,51869-36-4,51996-42-0,54656-60-9,57918-57-7,58769-79-2,62812-43-5,64429-66-9,67776-32-3,80483-26-7,97372-44-6
methyl 3-benzamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 93 percent / triphenylphosphine, diethyl azodicarboxylate

2: NBS / CHCl₃

3: 86 percent

4: tributyltin hydride

With N-Bromosuccinimide; tri-n-butyl-tin hydride; triphenylphosphine; diethylazodicarboxylate; In chloroform;
DOI:10.1039/c39850000352