(6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester

Base Information

• Chemical Name: (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester
• CAS No.: 68206-43-9
• Molecular Formula: C₂₆H₂₇N₅O₇S₂
• Molecular Weight: 585.662

Synonyms:

Chemical Property of (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester

Chemical Property:

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Technology Process of (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester

There total 1 articles about (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-nitro-2-pyridinesulfenyl chloride (68206-45-1) + (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid; sodium salt → (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester (68206-43-9)

Guidance literature:

With triphenylphosphine; In dichloromethane;

DOI:10.1246/cl.1978.979

Reference yield:

(6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carbothioic acid S-(3-nitro-pyridin-2-yl) ester (68206-43-9) + glycerol (56-81-5,25618-55-7,64333-26-2,8013-25-0) → (6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid (Ξ)-2,3-dihydroxy-propyl ester (68206-44-0)

Guidance literature:

With mercury(II) diacetate; In dichloromethane;

DOI:10.1246/cl.1978.979

upstream raw materials:

3-nitro-2-pyridinesulfenyl chloride

Downstream raw materials:

(6R)-7t-((R)-2-tert-butoxycarbonylamino-2-phenyl-acetylamino)-3-methyl-8-oxo-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid (Ξ)-2,3-dihydroxy-propyl ester

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