(E)-N-cyclopropylcinnamamide

Base Information

Chemical Name:(E)-N-cyclopropylcinnamamide
CAS No.:27845-66-5
Molecular Formula:C₁₂H₁₃NO
Molecular Weight:187.241
Hs Code.:

Synonyms:

Suppliers and Price of (E)-N-cyclopropylcinnamamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E)-N-cyclopropylcinnamamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E)-N-cyclopropylcinnamamide

There total 5 articles about (E)-N-cyclopropylcinnamamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 765-30-0
Cyclopropylamine

: 59831-96-8,27845-66-5
(E)-N-cyclopropylcinnamamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃; for 16h;
DOI:10.1002/anie.201907060

Reference yield:

: 140-10-3
(E)-3-phenylacrylic acid

: 765-30-0
Cyclopropylamine

: 59831-96-8,27845-66-5
(E)-N-cyclopropylcinnamamide

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 - 25 ℃; for 8h; Inert atmosphere;

Reference yield:

: 33603-90-6
(2Z)-2-bromo-3-phenyl-2-propenal

: 59831-96-8,27845-66-5
(E)-N-cyclopropylcinnamamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; caesium carbonate / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 6 h / 50 °C / Inert atmosphere

With 1,3-dibenzyl-1H-benzo[d]imidazol-3-ium chloride; caesium carbonate; In tetrahydrofuran;
DOI:10.1039/c2cc32862c