Technology Process of C37H47N7O3
There total 6 articles about C37H47N7O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
2: lithium hydroxide / tetrahydrofuran
3: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
With
triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; lithium hydroxide;
In
tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2012.02.066
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium tert-butylate / tert-butyl alcohol
2: palladium on activated charcoal; hydrogen / methanol; ethyl acetate
3: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
4: lithium hydroxide / tetrahydrofuran
5: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
With
palladium on activated charcoal; potassium tert-butylate; hydrogen; triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate; tert-butyl alcohol;
1: Stobbe condensation;
DOI:10.1016/j.bmcl.2012.02.066
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium on activated charcoal; hydrogen / methanol; ethyl acetate
2: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
3: lithium hydroxide / tetrahydrofuran
4: triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / dichloromethane
With
palladium on activated charcoal; hydrogen; triethylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; lithium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1016/j.bmcl.2012.02.066