1-acetamido-2-vinylcyclohexane

Base Information

• Chemical Name: 1-acetamido-2-vinylcyclohexane
• CAS No.: 132408-78-7
• Molecular Formula: C₁₀H₁₇NO
• Molecular Weight: 167.251
• Mol file: 132408-78-7.mol

Synonyms:

Chemical Property of 1-acetamido-2-vinylcyclohexane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-acetamido-2-vinylcyclohexane

There total 8 articles about 1-acetamido-2-vinylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethylidenecyclohexane (1003-64-1) → 1-acetamido-2-vinylcyclohexane (132408-78-7)

Guidance literature:

Multi-step reaction with 3 steps

1: 6 percent / benzene / 18 h / 40 °C

2: 1) Zn-dust, glacial acetic acid / acetone / Ambient temperature; 1) 15 min 2) 1 h

3: pyridine / CH₂Cl₂ / 18 h / Ambient temperature

With pyridine; acetic acid; zinc; In dichloromethane; acetone; benzene;

DOI:10.1021/jo00005a063

Reference yield:

C14H18Cl6N2O4 → 1-acetamido-2-vinylcyclohexane (132408-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 1) Zn-dust, glacial acetic acid / acetone / Ambient temperature; 1) 15 min 2) 1 h

2: pyridine / CH₂Cl₂ / 18 h / Ambient temperature

With pyridine; acetic acid; zinc; In dichloromethane; acetone;

DOI:10.1021/jo00005a063

Reference yield:

acetic anhydride (108-24-7) + amino-1 vinyl-1 cyclohexane (111709-87-6) → 1-acetamido-2-vinylcyclohexane (132408-78-7)

Guidance literature:

With pyridine; In dichloromethane; for 18h; Yield given; Ambient temperature;

DOI:10.1021/jo00005a063

upstream raw materials:

acetic anhydride

amino-1 vinyl-1 cyclohexane

ethylidenecyclohexane

ethyl cyclohexylideneacetate