benzoylacetonato-bis(cyclopentadienyl)titanium(IV) bromide

Base Information

• Chemical Name: benzoylacetonato-bis(cyclopentadienyl)titanium(IV) bromide
• CAS No.: 86407-63-8
• Molecular Formula: Br*C₂₀H₁₉O₂Ti
• Molecular Weight: 419.154
• Mol file: 86407-63-8.mol

Synonyms:

Chemical Property of benzoylacetonato-bis(cyclopentadienyl)titanium(IV) bromide

Chemical Property:

Purity/Quality:

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Technology Process of benzoylacetonato-bis(cyclopentadienyl)titanium(IV) bromide

There total 1 articles about benzoylacetonato-bis(cyclopentadienyl)titanium(IV) bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

bis(cyclopentadienyl)titanium dichloride (1271-19-8) + 1-phenylbutan-1,3-dione (93-91-4) + potassium bromide (7558-02-3,7758-02-3) → benzoylacetonato-bis(cyclopentadienyl)titanium(IV) bromide (86407-63-8)

Guidance literature:

In water; to an aq. soln. of Ti-compd. benzoylacetone is added, mixt. is stirred for 2 h, this soln. is added to a hot aq. soln. of KBr; ppt. is digested on a water-bath for 2 h, collected on a glass frit andwashed several times with ether, ppt. is recrystd. from methanol, elem.anal.;

upstream raw materials:

bis(cyclopentadienyl)titanium dichloride

1-phenylbutan-1,3-dione

potassium bromide