Au₂Re₂H₇⁽¹⁺⁾6(P(C₆H₅)3)BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄

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Chemical Name:Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄
CAS No.:117201-67-9
Molecular Formula:BF₄*6C₁₈H₁₅P*Au₂H₇Re₂
Molecular Weight:2433.95
Hs Code.:

Au<sub>2</sub>Re<sub>2</sub>H<sub>7</sub><sup>(1+)</sup>*6(P(C<sub>6</sub>H<sub>5</sub>)3)*BF<sub>4</sub><sup>(1-)</sup>=Au<sub>2</sub>Re<sub>2</sub>H<sub>7</sub>(P(C<sub>6</sub>H<sub>5</sub>)3)6BF<sub>4</sub>

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Chemical Property of Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄

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Technology Process of Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄

There total 2 articles about Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Au₂Re₂H₇⁽²⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)*PF₆^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6(BF₄)(PF₆)

: 117201-67-9
Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄

Guidance literature:: With H₂; In acetonitrile; Au-Re-complex in CH3CN was stirred under 1 atm H2 for 3 h, upon addn. of ether a brown ppt. was formed.; identified UV-spect.;

Reference yield:

: 53317-87-6
tris[triphenylphosphinegold(I)]oxonium tetrafluoroborate

: 66984-37-0
Re₂H₈*4(P(C₆H₅)3)=Re₂H₈(P(C₆H₅)3)4

: AuRe₂H₇*5(P(C₆H₅)3)

: 117201-67-9
Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄

Guidance literature:: In dichloromethane; degassed Re- and Au-complex were dissolved in freshly distd. CH2Cl2, forming a dark-red soln. which on treating with ether formed a red-brown solid.; solid Au2Re2H7(PPh3)6BF4 was washed with ether; elem. anal. In the mother liquor remained AuRe2H7(PPh3)5, not isolated.;

Reference yield:

: 117201-67-9
Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)*BF₄^(1-)=Au₂Re₂H₇(P(C₆H₅)3)6BF₄

: Au₂Re₂H₆⁽¹⁺⁾*6(P(C₆H₅)3)=(Au₂Re₂H₆(P(C₆H₅)3)6)⁽¹⁺⁾

: Au₂Re₂H₆*6(P(C₆H₅)3)=Au₂Re₂H₆(P(C₆H₅)3)6

Guidance literature:: With KOC(CH₃)3; In tetrahydrofuran; Au-Re complex and KO-tert-Bu were dissolved in THF and stirred for 1 h, then solvent was removed in vac.; the residue was extd. with toluene-d8.; not isolated, detected by NMR.;