Fe(5,10,15,20-tetraphenylporphine)CO(4-acetoxypyridine)

Base Information

• Chemical Name: Fe(5,10,15,20-tetraphenylporphine)CO(4-acetoxypyridine)
• CAS No.: 109434-17-5
• Molecular Formula: C₅₂H₃₇FeN₅O₃
• Molecular Weight: 835.744
• Mol file: 109434-17-5.mol

Synonyms:

Chemical Property of Fe(5,10,15,20-tetraphenylporphine)CO(4-acetoxypyridine)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of Fe(5,10,15,20-tetraphenylporphine)CO(4-acetoxypyridine)

There total 1 articles about Fe(5,10,15,20-tetraphenylporphine)CO(4-acetoxypyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-acetoxypyridine (14210-20-9) + 5,10,15,20-tetraphenyl-21H,23H-porphine (917-23-7,20998-75-8) + iron(II) acetate (1834-30-6,2140-52-5,3094-87-9) → Fe(5,10,15,20-tetraphenylporphine)CO(4-acetoxypyridine) (109434-17-5)

Guidance literature:

With carbon monoxide; In chloroform; acetic acid; a soln. of Fe(CH3COO)2 in CH3COOH was added dropwise to soln. of ligand and excess of 4-acetoxypyridine in chloroform, the mixt. was heated at 57°C for 2.5 h, then the temp. was reduced to 0°C, CO slowly bubbled through the soln. for 1 h; the soln. was sealed under CO and refrigerated overnight, ppt. was collected by filtration, washed with Et2O, dried under vac. at ambient temp.; elem. anal.;

upstream raw materials:

4-acetoxypyridine

5,10,15,20-tetraphenyl-21H,23H-porphine

iron(II) acetate