4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

Base Information

Chemical Name:4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole
CAS No.:1038692-16-8
Molecular Formula:C₂₅H₁₅F₅N₄
Molecular Weight:466.413
Hs Code.:

Synonyms:

Suppliers and Price of 4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

There total 1 articles about 4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 653-37-2
perfluorobenzaldehyde

: 51802-04-1
N,N'-dibenzyldiaminomaleonitrile

: 1038692-16-8
4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

Guidance literature:: In acetic acid; at 20 ℃; for 48h;
DOI:10.1016/j.jorganchem.2008.01.039

Reference yield: 43.0%

: 1038692-16-8
4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

: carbonylchloro(1,3-dibenzyl-4,5-dicyano-1H-imidazolin-2-ylidene)rhodium(I) dimer

: trans-carbonylchlorobis(1,3-dibenzyl-4,5-dicyano-1H-imidazolin-2-ylidene)rhodium(I)

Guidance literature:: In 1,3,5-trimethyl-benzene; (N2); addn. of 1 equiv. of (RhCl(CO)(C3(CN)2N2(CH2C6H5)2))2 to 2 equiv. of 4,5-dicyano-1,3-dibenzyl-2-pentafluorophenyl-2,3-dihydroimidazole in mesitylene at 165°C; stirring for 6 h; removal of solvent in vac., chromy. using silica as stationary phase andCH2Cl2 as eluent; drying under reduced pressure; elem. anal.;
DOI:10.1021/om900785p

Reference yield:

: 1038692-16-8
4,5-dicyano-1,3-dibenzyl-2-(pentafluorophenyl)-2,3-dihydroimidazole

: carbonylchloro(1,3-dibenzyl-4,5-dichloro-1H-imidazolin-2-ylidene)rhodium(I) dimer

: trans-carbonylchlorobis(1,3-dibenzyl-4,5-dichloro-1H-imidazolin-2-ylidene)rhodium(I)

: trans-carbonylchloro-1,3-dibenzyl-4,5-dichloro-1H-imidazolin-2-ylidene-1,3-dibenzyl-4,5-dicyano-1H-imidazolin-2-ylidenerhodium(I)

Guidance literature:: In 1,3,5-trimethyl-benzene; (N2); addn. of 1 equiv. of (RhCl(CO)(C3Cl2N2(CH2C6H5)2))2 to 2 equiv. of4,5-dicyano-1,3-dibenzyl-2-pentafluorophenyl-2,3-dihydroimidazole in me sitylene at 165°C; stirring for 6 h; removal of solvent in vac., chromy. using silica as stationary phase andCH2Cl2 as eluent; drying under reduced pressure; as mixt.;
DOI:10.1021/om900785p