Os(P(C₆H₅)3)3Cl₂

Base Information

Chemical Name:Os(P(C₆H₅)3)3Cl₂
CAS No.:56586-93-7
Molecular Formula:C₅₄H₄₅Cl₂OsP₃
Molecular Weight:1047.98
Hs Code.:

Os(P(C<sub>6</sub>H<sub>5</sub>)3)3Cl<sub>2</sub>

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Os(P(C₆H₅)3)3Cl₂

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Technology Process of Os(P(C₆H₅)3)3Cl₂

There total 10 articles about Os(P(C₆H₅)3)3Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: potassium osmate

: 603-35-0
triphenylphosphine

: 56586-93-7,40802-32-2
dichlorotris(triphenylphosphine)osmium(II)

Guidance literature:: In water; tert-butyl alcohol; (under Ar); soln. of K2OsO2(OH)4 in conc. HCl heated at reflux for 18 h,evapd., P(C6H5)3 in t-butanol and water added, refluxed for 18 h, coole d; filtered, washed with EtOH and hexane, dried in vac.;
DOI:10.1016/j.ica.2005.09.070

Reference yield: 92.0%

: diammonium hexachloroosmate(IV)

: 603-35-0
triphenylphosphine

: 56586-93-7,40802-32-2
dichlorotris(triphenylphosphine)osmium(II)

Guidance literature:: In 2-methoxy-ethanol; water; refluxing mixt. of osmium compd. and phosphine deriv. in 5:2 methoxyethanol/water for 3 h under Ar; cooling to room temp., filtration, washing with water, methanol and diethyl ether, drying in air;
DOI:10.1021/ic9020178

Reference yield: 92.0%

: diammonium hexachloroosmate(IV)

: 56586-93-7,40802-32-2
dichlorotris(triphenylphosphine)osmium(II)

Guidance literature:: With triphenylphosphine; In water; tert-butyl alcohol; Os complex and PPh3 refluxing in aq. t-BuOH for 90 h under N2, cooling,ppt. filtering off, washing with water, MeOH and Et2O, drying in vacuo; identified by elem. anal., IR and NMR spectra;
DOI:10.1016/S0020-1693(00)83666-X