N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

Base Information

Chemical Name:N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide
CAS No.:109923-80-0
Molecular Formula:C₂₉H₄₅N₃O₇Si₂
Molecular Weight:603.863
Hs Code.:

N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

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Chemical Property of N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

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Technology Process of N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

There total 9 articles about N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3080-30-6,6974-32-9,14215-97-5,16162-35-9,20822-87-1,21138-42-1,22249-15-6,22249-17-8,26287-72-9,53403-35-3,53403-36-4,57236-69-8,70832-64-3,99395-04-7,100101-51-7,109668-83-9,120019-54-7
1-O-acetyl-2,3,5-tri-O-benzoyl-β-L-ribofuranose

: 109923-80-0
N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: 2.) trimethylsylil triflate / 1.) 1,2-dichloroethane, toluene, reflux, 30 min, 2.) 1 h

2: 71 percent / pyridine; dioxane / 1 h

3: sodium methoxide / pyridine / 0.17 h

4: pyridine / 1 h

With trimethylsilyl trifluoromethanesulfonate; sodium methylate; In 1,4-dioxane; pyridine;

Reference yield:

: 41546-19-4
α-L-lyxose

: 109923-80-0
N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

Guidance literature:: Multi-step reaction with 7 steps

1: HCl / 4 h

2: 90 percent / CH₂Cl₂; pyridine / 3 h

3: 9.5 g / sulphuric acid, acetic acid / 15 h / 0 - 5 °C

4: 2.) trimethylsylil triflate / 1.) 1,2-dichloroethane, toluene, reflux, 30 min, 2.) 1 h

5: 71 percent / pyridine; dioxane / 1 h

6: sodium methoxide / pyridine / 0.17 h

7: pyridine / 1 h

With hydrogenchloride; trimethylsilyl trifluoromethanesulfonate; sulfuric acid; sodium methylate; acetic acid; In 1,4-dioxane; pyridine; dichloromethane;

Reference yield:

: 933-88-0
ortho-toluoyl chloride

: 109923-80-0
N-[1-((2S,3S,3aR,9aS)-3-Hydroxy-5,5,7,7-tetraisopropyl-tetrahydro-1,4,6,8-tetraoxa-5,7-disila-cyclopentacycloocten-2-yl)-2-oxo-1,2-dihydro-pyrimidin-4-yl]-2-methyl-benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / pyridine; dioxane / 1 h

2: sodium methoxide / pyridine / 0.17 h

3: pyridine / 1 h

With sodium methylate; In 1,4-dioxane; pyridine;