((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane

Base Information

• Chemical Name: ((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane
• CAS No.: 1286212-12-1
• Molecular Formula: C₂₂H₄₄OSi
• Molecular Weight: 352.676
• Mol file: 1286212-12-1.mol

Synonyms:

Chemical Property of ((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of ((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane

There total 2 articles about ((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclohexenone (930-68-7) + 2-bromoheptane (1974-04-5) + chlorotripropylsilane (995-25-5) → ((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane (1286212-12-1)

Guidance literature:

With manganese; (1,2-dimethoxyethane)dichloronickel(II); 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; In N,N-dimethyl-formamide; at 40 ℃; for 24h; Inert atmosphere;

DOI:10.1021/ol200881v

Reference yield:

cyclohexenone (930-68-7) + 2-iodoheptane (18589-29-2) + chlorotripropylsilane (995-25-5) → ((3-(heptan-2-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane (1286212-12-1) + ((3-(heptan-3-yl)cyclohex-1-en-1-yl)oxy)tripropylsilane (1286212-38-1)

Guidance literature:

With bis(acetylacetonate)nickel(II); manganese; 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; In N,N-dimethyl-formamide; at 40 ℃; for 2h;

DOI:10.1021/ol200881v

upstream raw materials:

cyclohexenone

2-iodoheptane

chlorotripropylsilane

2-bromoheptane

Refernces