[(((C₆H₅CH₂)NCH₂CH₂)2CH₂CH₂CH₂N(CH₂C₆H₅))Cu(CH₃CN)]⁽¹⁺⁾*SbF₆^(1-)=[(((C₆H₅CH₂)NCH₂CH₂)2(CH₂)3N(CH₂C₆H₅))Cu(CH₃CN)]SbF₆

Base Information

• Chemical Name: [(((C₆H₅CH₂)NCH₂CH₂)2CH₂CH₂CH₂N(CH₂C₆H₅))Cu(CH₃CN)]⁽¹⁺⁾*SbF₆^(1-)=[(((C₆H₅CH₂)NCH₂CH₂)2(CH₂)3N(CH₂C₆H₅))Cu(CH₃CN)]SbF₆
• CAS No.: 296761-84-7
• Molecular Formula: C₃₀H₃₈CuN₄*F₆Sb
• Molecular Weight: 753.945

Synonyms:

Chemical Property of [(((C₆H₅CH₂)NCH₂CH₂)2CH₂CH₂CH₂N(CH₂C₆H₅))Cu(CH₃CN)]⁽¹⁺⁾*SbF₆^(1-)=[(((C₆H₅CH₂)NCH₂CH₂)2(CH₂)3N(CH₂C₆H₅))Cu(CH₃CN)]SbF₆

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Technology Process of [(((C₆H₅CH₂)NCH₂CH₂)2CH₂CH₂CH₂N(CH₂C₆H₅))Cu(CH₃CN)]⁽¹⁺⁾*SbF₆^(1-)=[(((C₆H₅CH₂)NCH₂CH₂)2(CH₂)3N(CH₂C₆H₅))Cu(CH₃CN)]SbF₆

There total 1 articles about [(((C₆H₅CH₂)NCH₂CH₂)2CH₂CH₂CH₂N(CH₂C₆H₅))Cu(CH₃CN)]⁽¹⁺⁾*SbF₆^(1-)=[(((C₆H₅CH₂)NCH₂CH₂)2(CH₂)3N(CH₂C₆H₅))Cu(CH₃CN)]SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

[Cu(acetonitrile)4]SbF6 (137436-76-1) + 1,4,7-triphenyl-1,4,7-triazacyclodecane (296761-75-6) → [(((C6H5CH2)NCH2CH2)2CH2CH2CH2N(CH2C6H5))Cu(CH3CN)](1+)*SbF6(1-)=[(((C6H5CH2)NCH2CH2)2(CH2)3N(CH2C6H5))Cu(CH3CN)]SbF6 (296761-84-7)

Guidance literature:

In dichloromethane; inert-atm. glovebox; solid Cu complex added to stirred soln. of ligand in CH3CN; stirred for 10 min; Et2O added; pptd.; recrystd. (CH2Cl2/Et2O, 1/20); elem. anal.;

DOI:10.1021/ic000248p

Reference yield: 91.0%

[(((C6H5CH2)NCH2CH2)2CH2CH2CH2N(CH2C6H5))Cu(CH3CN)](1+)*SbF6(1-)=[(((C6H5CH2)NCH2CH2)2(CH2)3N(CH2C6H5))Cu(CH3CN)]SbF6 (296761-84-7) + carbon monoxide (201230-82-2) → [(((C6H5CH2)NCH2CH2)2CH2CH2CH2N(CH2C6H5))Cu(CO)](1+)*SbF6(1-)=[(((C6H5CH2)NCH2CH2)2(CH2)3N(CH2C6H5))Cu(CO)]SbF6 (296761-92-7)

Guidance literature:

In acetone; Standard Schlenk technique; CO bubbled through soln. of Cu complex in acetone for 5 min; soln. was allowed to equilibrate for 10 min; solvent removed under reduced pressure; recrystd. (acetone/Et2O, 1/20);elem. anal.;

DOI:10.1021/ic000248p

Reference yield:

[(((C6H5CH2)NCH2CH2)2CH2CH2CH2N(CH2C6H5))Cu(CH3CN)](1+)*SbF6(1-)=[(((C6H5CH2)NCH2CH2)2(CH2)3N(CH2C6H5))Cu(CH3CN)]SbF6 (296761-84-7) + oxygen (80937-33-3) → [(1,4,7-triphenyl-1,4,7-triazacyclodecane)2Cu2(μ-O)2](SbF6)2

Guidance literature:

In tetrahydrofuran; dry O2 bubbled through soln. of Cu complex in THF for 5 min at -80°C; UV-monitoring;

DOI:10.1021/ic000248p

upstream raw materials:

[Cu(acetonitrile)4]SbF₆

1,4,7-triphenyl-1,4,7-triazacyclodecane

Downstream raw materials:

[(((C₆H₅CH₂)NCH₂CH₂)2CH₂CH₂CH₂N(CH₂C₆H₅))Cu(CO)]⁽¹⁺⁾*SbF₆^(1-)=[(((C₆H₅CH₂)NCH₂CH₂)2(CH₂)3N(CH₂C₆H₅))Cu(CO)]SbF₆

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