[Co(PPh₃)2(CO)2Cl]

Base Information

Chemical Name:[Co(PPh₃)2(CO)2Cl]
CAS No.:133160-49-3
Molecular Formula:C₃₈H₃₀ClCoO₂P₂
Molecular Weight:675.049
Hs Code.:

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Chemical Property of [Co(PPh₃)2(CO)2Cl]

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Technology Process of [Co(PPh₃)2(CO)2Cl]

There total 3 articles about [Co(PPh₃)2(CO)2Cl] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: Cl^(1-)*Co⁽¹⁺⁾*2P(C₆H₅)3=ClCo(P(C₆H₅)3)2

: 133160-49-3,116558-66-8,14564-33-1
[Co(PPh₃)2(CO)2Cl]

Guidance literature:: With CO; In ethanol; under inert atm., CO was bubbled through a freshly prepared brown suspn. of Co-polymer in EtOH (stirred, room temp., 2 h), yellow orange suspn.; filtration, recrystn. (CH2Cl2/EtOH);
DOI:10.1016/0022-328X(86)82057-5

Reference yield:

: 101702-01-6
Cl^(1-)*Co⁽¹⁺⁾*P(C₆H₅)3=ClCo(P(C₆H₅)3)

: 133160-49-3,116558-66-8,14564-33-1
[Co(PPh₃)2(CO)2Cl]

Guidance literature:: With CO; In ethanol; under inert atm., CO was bubbled through brown suspn. of Co-polymer in EtOH (stirred, room temp., 2 h); solid filtered off, extn. (CH2Cl2), addn. of EtOH;
DOI:10.1016/0022-328X(86)82057-5

Reference yield:

: Na⁽¹⁺⁾*{Co(CO)3P(C₆H₅)3}^(1-)*C₄H₈O=Na{Co(CO)3P(C₆H₅)3}*C₄H₈O

: 10025-87-3,12599-09-6,63736-95-8,39380-77-3
trichlorophosphate

: 133160-49-3,116558-66-8,14564-33-1
[Co(PPh₃)2(CO)2Cl]

Guidance literature:: In tetrahydrofuran; byproducts: CO; addn. of POCl3 at -70 °C, substitution reaction at -50 °C;; product precipitates after 1 h, washed with methanol and water;;