hexameric n-butyloxotin p-chlorobenzoate

Base Information

• Chemical Name: hexameric n-butyloxotin p-chlorobenzoate
• CAS No.: 115270-28-5
• Molecular Formula: C₆₆H₇₈Cl₆O₁₈Sn₆
• Molecular Weight: 2084.31
• Mol file: 115270-28-5.mol

Synonyms:

Chemical Property of hexameric n-butyloxotin p-chlorobenzoate

Chemical Property:

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Safty Information:

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Technology Process of hexameric n-butyloxotin p-chlorobenzoate

There total 1 articles about hexameric n-butyloxotin p-chlorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.3%

n-butylstannoic acid (2273-43-0) + para-chlorobenzoic acid (74-11-3) → hexameric n-butyloxotin p-chlorobenzoate (115270-28-5)

Guidance literature:

In benzene; byproducts: water; addn. of Cl-p-C6H4COOH to n-butylstannoic acid in dry benzene, heating (reflux, 4 h), removal of water (azeotropic distn., Dean-Stark app.); removal of solvent (vac.), soln. of solid in hot benzene/hexane, keeping in the refrigerator; elem. anal.;

upstream raw materials:

n-butylstannoic acid

para-chlorobenzoic acid

Refernces