Au₂Re₂H₈⁽²⁺⁾6(P(C₆H₅)3)2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2

Base Information

Chemical Name:Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2
CAS No.:117201-66-8
Molecular Formula:2BF₄*6C₁₈H₁₅P*Au₂H₈Re₂
Molecular Weight:2521.76
Hs Code.:

Au<sub>2</sub>Re<sub>2</sub>H<sub>8</sub><sup>(2+)</sup>*6(P(C<sub>6</sub>H<sub>5</sub>)3)*2BF<sub>4</sub><sup>(1-)</sup>=Au<sub>2</sub>Re<sub>2</sub>H<sub>8</sub>(P(C<sub>6</sub>H<sub>5</sub>)3)6(BF<sub>4</sub>)2

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Chemical Property of Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2

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Technology Process of Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2

There total 1 articles about Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.6%

: 67969-82-8
tetrafluoroboric acid diethyl ether

: Au₂Re₂H₆*6(P(C₆H₅)3)=Au₂Re₂H₆(P(C₆H₅)3)6

: 117201-66-8
Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2

Guidance literature:: In dichloromethane; toluene; soln. of Au-Re complex in toluene was treated with HBF4*Et2O resulting an oil from which solvents were removed in vac.; residue was extd. with CH2Cl2 and pptd. with ether.; residue was washed with ether.;

Reference yield:

: 117201-66-8
Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2

: 47807-21-6
bis(triphenylphosphine)gold(I)(1+)

: Au₂Re₂H₇⁽¹⁺⁾*6(P(C₆H₅)3)=(Au₂Re₂H₇(P(C₆H₅)3)6)⁽¹⁺⁾

Guidance literature:: In diethyl ether; dichloromethane; decompn. at attempts to recrystallize the Au-Re complex; formation of other uncharacterized P-compds.;

Reference yield:

: 117201-66-8
Au₂Re₂H₈⁽²⁺⁾*6(P(C₆H₅)3)*2BF₄^(1-)=Au₂Re₂H₈(P(C₆H₅)3)6(BF₄)2

: 38011-35-7
bis(triphenylphosphine)iminium nitrate

: Au₂Re₂H₆⁽¹⁺⁾*6(P(C₆H₅)3)=(Au₂Re₂H₆(P(C₆H₅)3)6)⁽¹⁺⁾

Guidance literature:: In dichloromethane; Au-Re-complex and 2 equiv. of (PPN)NO3 were dissolved in CH2Cl2, wthin several min color changed to blue-green; not isolated, detected UV-spect.;