[(η5C5Me5)FeH(1,3-bis(diphenylphosphino)propane)][PF6]

Base Information

• Chemical Name: [(η5C5Me5)FeH(1,3-bis(diphenylphosphino)propane)][PF6]
• CAS No.: 420796-93-6
• Molecular Formula: C₃₇H₄₂FeP₂*F₆P
• Molecular Weight: 749.499
• Mol file: 420796-93-6.mol

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Chemical Property of [(η5C5Me5)FeH(1,3-bis(diphenylphosphino)propane)][PF6]

Chemical Property:

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Technology Process of [(η5C5Me5)FeH(1,3-bis(diphenylphosphino)propane)][PF6]

There total 1 articles about [(η5C5Me5)FeH(1,3-bis(diphenylphosphino)propane)][PF6] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

ferrocenium hexafluorophosphate + [(η5-C5Me5)Fe(1,3-bis(diphenylphosphino)propane)H] (420796-88-9) → [(η5C5Me5)FeH(1,3-bis(diphenylphosphino)propane)][PF6] (420796-93-6)

Guidance literature:

In tetrahydrofuran; (C5H5)2FEPF6 was added to THF soln. of complex at 20°C, stirred for 1 h (inert atm.); reduced in vol., pentane was added, ppt. was filtered, washed with diethyl ether, crystd. from THF-pentane; elem. anal.;

DOI:10.1021/om0108245

upstream raw materials:

[(η5-C5Me5)Fe(1,3-bis(diphenylphosphino)propane)H]