Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester
CAS No.:78959-15-6
Molecular Formula:C₁₃H₁₇N₃O₂S
Molecular Weight:279.363
Hs Code.:
DSSTox Substance ID:DTXSID20229418
Wikidata:Q83109655

Synonyms:BRN 4503841;Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester;1,1-Dimethylethyl 2-(2H-1,4-benzothiazin-3-yl)hydrazinecarboxylate;78959-15-6;C13H17N3O2S;DTXSID20229418;LS-76667

Suppliers and Price of Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester

Chemical Property:

Density:1.26g/cm³
XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:279.10414797
Heavy Atom Count:19
Complexity:365

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)OC(=O)NNC1=NC2=CC=CC=C2SC1

Technology Process of Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester

There total 3 articles about Hydrazinecarboxylic acid, 2-(2H-1,4-benzothiazin-3-yl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 72223-33-7
3-(methylthio)-2H-1,4-benzothiazine

: 870-46-2
t-butoxycarbonylhydrazine

: 78959-15-6
N'-(2H-Benzo[1,4]thiazin-3-yl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: In ethanol; Ambient temperature;

Reference yield:

: 22191-30-6
2H-1,4-benzothiazine-3(4H)-thione

: 78959-15-6
N'-(2H-Benzo[1,4]thiazin-3-yl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / 8 h / Heating

2: 58 percent / ethanol / Ambient temperature

With potassium carbonate; In ethanol; acetone;

Reference yield:

: 5325-20-2
2H-1,4-benzothiazin-3-one

: 78959-15-6
N'-(2H-Benzo[1,4]thiazin-3-yl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / P₂S₅/Et₃N / acetonitrile

2: K₂CO₃ / acetone / 8 h / Heating

3: 58 percent / ethanol / Ambient temperature

With tetraphosphorus decasulfide; potassium carbonate; triethylamine; In ethanol; acetone; acetonitrile;