Technology Process of C29H39NO9
There total 7 articles about C29H39NO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / 1 h / 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere; Cooling with ice
2.2: 0 - 20 °C / Inert atmosphere
3.1: sodium hydroxide; water / methanol / 4 h / 60 °C
4.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / Inert atmosphere
With
dmap; thionyl chloride; water; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; mineral oil;
DOI:10.1002/psc.2459
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogenchloride; zinc amalgam / water / Reflux
2.1: thionyl chloride / 1 h / 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere; Cooling with ice
3.2: 0 - 20 °C / Inert atmosphere
4.1: sodium hydroxide; water / methanol / 4 h / 60 °C
5.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / Inert atmosphere
With
hydrogenchloride; dmap; thionyl chloride; zinc amalgam; water; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; mineral oil;
1.1: |Clemmensen Reduction;
DOI:10.1002/psc.2459
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: aluminum (III) chloride / dichloromethane / -20 - 20 °C
2.1: hydrogenchloride; zinc amalgam / water / Reflux
3.1: thionyl chloride / 1 h / 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere; Cooling with ice
4.2: 0 - 20 °C / Inert atmosphere
5.1: sodium hydroxide; water / methanol / 4 h / 60 °C
6.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / Inert atmosphere
With
hydrogenchloride; dmap; aluminum (III) chloride; thionyl chloride; zinc amalgam; water; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water; mineral oil;
1.1: |Friedel-Crafts Acylation / 2.1: |Clemmensen Reduction;
DOI:10.1002/psc.2459