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C29H39NO9

Base Information
  • Chemical Name:C29H39NO9
  • CAS No.:1417703-02-6
  • Molecular Formula:C29H39NO9
  • Molecular Weight:545.63
  • Hs Code.:
C<sub>29</sub>H<sub>39</sub>NO<sub>9</sub>

Synonyms:

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Chemical Property of C29H39NO9
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Technology Process of C29H39NO9

There total 7 articles about C29H39NO9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1.1: thionyl chloride / 1 h / 20 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere; Cooling with ice
2.2: 0 - 20 °C / Inert atmosphere
3.1: sodium hydroxide; water / methanol / 4 h / 60 °C
4.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / Inert atmosphere
With dmap; thionyl chloride; water; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; mineral oil;
DOI:10.1002/psc.2459
Guidance literature:
Multi-step reaction with 5 steps
1.1: hydrogenchloride; zinc amalgam / water / Reflux
2.1: thionyl chloride / 1 h / 20 °C
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere; Cooling with ice
3.2: 0 - 20 °C / Inert atmosphere
4.1: sodium hydroxide; water / methanol / 4 h / 60 °C
5.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / Inert atmosphere
With hydrogenchloride; dmap; thionyl chloride; zinc amalgam; water; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; mineral oil; 1.1: |Clemmensen Reduction;
DOI:10.1002/psc.2459
Guidance literature:
Multi-step reaction with 6 steps
1.1: aluminum (III) chloride / dichloromethane / -20 - 20 °C
2.1: hydrogenchloride; zinc amalgam / water / Reflux
3.1: thionyl chloride / 1 h / 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / Inert atmosphere; Cooling with ice
4.2: 0 - 20 °C / Inert atmosphere
5.1: sodium hydroxide; water / methanol / 4 h / 60 °C
6.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / Inert atmosphere
With hydrogenchloride; dmap; aluminum (III) chloride; thionyl chloride; zinc amalgam; water; sodium hydride; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; mineral oil; 1.1: |Friedel-Crafts Acylation / 2.1: |Clemmensen Reduction;
DOI:10.1002/psc.2459
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