(1,3-dichloro-2-azulenyl)diphenylbismuth difluoride

Base Information

• Chemical Name: (1,3-dichloro-2-azulenyl)diphenylbismuth difluoride
• CAS No.: 827347-46-6
• Molecular Formula: C₂₂H₁₅BiCl₂F₂
• Molecular Weight: 597.244
• Mol file: 827347-46-6.mol

Synonyms:

Chemical Property of (1,3-dichloro-2-azulenyl)diphenylbismuth difluoride

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (1,3-dichloro-2-azulenyl)diphenylbismuth difluoride

There total 1 articles about (1,3-dichloro-2-azulenyl)diphenylbismuth difluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

xenon difluoride (13709-36-9) + (1,3-dichloro-2-azulenyl)diphenylbismuthane (827347-43-3) → (1,3-dichloro-2-azulenyl)diphenylbismuth difluoride (827347-46-6)

Guidance literature:

In tetrahydrofuran; under Ar atm. to soln. Bi compound in THF XeF2 was added at 0°C, react. mixt. was stirred for 3 h; soln. was evapd., residue was crystd. from MeOH; elem. anal.;

DOI:10.1021/om040053f

upstream raw materials:

xenon difluoride

(1,3-dichloro-2-azulenyl)diphenylbismuthane