1,4-Dichloro-2-(trichloromethyl)benzene

Base Information

• Chemical Name: 1,4-Dichloro-2-(trichloromethyl)benzene
• CAS No.: 10541-71-6
• Molecular Formula: C7H3Cl5
• Molecular Weight: 264.366
• Hs Code.: 2903999090
• European Community (EC) Number: 234-120-1
• DSSTox Substance ID: DTXSID50147116
• Nikkaji Number: J140.755D
• Wikidata: Q83012198
• Mol file: 10541-71-6.mol

Synonyms:1,4-Dichloro-2-(trichloromethyl)benzene;10541-71-6;EINECS 234-120-1;Benzene,1,4-dichloro-2-(trichloromethyl)-;SCHEMBL7943012;DTXSID50147116;Benzene, 1,4-dichloro-2-(trichloromethyl)-

Chemical Property of 1,4-Dichloro-2-(trichloromethyl)benzene

Chemical Property:

• Vapor Pressure: 0.00547mmHg at 25°C
• Refractive Index: 1.583
• Boiling Point: 283.3 °C at 760 mmHg
• Flash Point: 126.5 °C
• PSA: 0.00000
• Density: 1.605 g/cm³
• LogP: 4.82010
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 263.864788
• Heavy Atom Count: 12
• Complexity: 152

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,4-DICHLORO-2-(TRICHLOROMETHYL)BENZENE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C=C1Cl)C(Cl)(Cl)Cl)Cl

Technology Process of 1,4-Dichloro-2-(trichloromethyl)benzene

There total 6 articles about 1,4-Dichloro-2-(trichloromethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-dichlorobenzene (106-46-7,84348-21-0) → 1,4-dichloro-2-trichloromethyl-benzene (10541-71-6) + dichloro-bis-(2,5-dichloro-phenyl)-methane

Guidance literature:

With tetrachloromethane; C₆H₁₁N₂⁽¹⁺⁾*Cl^(1-)*AlCl₃; at 60 ℃; for 2h; under 760.051 Torr;

DOI:10.1007/s10562-018-2633-8

Reference yield:

2,6-dichlorobenzalchloride (81-19-6) → 1,4-dichloro-2-trichloromethyl-benzene (10541-71-6)

Guidance literature:

Reference yield:

dichlorophosphoric acid-(4-chloro-2-trichloromethyl-phenyl ester) → 1,4-dichloro-2-trichloromethyl-benzene (10541-71-6)

Guidance literature:

With phosphorus pentachloride; at 210 - 220 ℃; im geschlossenen Rohr;

upstream raw materials:

chloroform

2,6-dichlorobenzalchloride

para-dichlorobenzene

Downstream raw materials:

2,5-dichlorobenzoic acid

Refernces

• 1、 -. "Process for stripping and distilling mixtures containing alkylaromatics chlorinated in the side chain". . . Retrieved 2008/06/13.