Technology Process of C29H42N2O9
There total 4 articles about C29H42N2O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
diethyl 2-benzyloxycarbonylaminomalonate;
With
caesium carbonate;
In
N,N-dimethyl-formamide;
for 0.5h;
Cooling with ice;
Inert atmosphere;
C14H24INO3;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 8h;
Inert atmosphere;
DOI:10.1039/c3cc42365d
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere
2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere
2.2: 8 h / 20 °C / Inert atmosphere
With
1H-imidazole; iodine; caesium carbonate; triphenylphosphine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42365d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 3 h / 20 °C / Cooling with ice; Inert atmosphere
2.1: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / Cooling with ice; Inert atmosphere
3.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Cooling with ice; Inert atmosphere
3.2: 8 h / 20 °C / Inert atmosphere
With
1H-imidazole; tetrabutyl ammonium fluoride; iodine; caesium carbonate; triphenylphosphine;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3cc42365d
