[PdClO₄(C₅H₄N)(P(C₆H₅)3)]2

Base Information

• Chemical Name: [PdClO₄(C₅H₄N)(P(C₆H₅)3)]2
• CAS No.: 90752-08-2
• Molecular Formula: C₄₆H₃₈Cl₂N₂O₈P₂Pd₂
• Molecular Weight: 1092.51

Synonyms:

Chemical Property of [PdClO₄(C₅H₄N)(P(C₆H₅)3)]2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [PdClO₄(C₅H₄N)(P(C₆H₅)3)]2

There total 1 articles about [PdClO₄(C₅H₄N)(P(C₆H₅)3)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

[PdBr(C5H4N)(P(C6H5)3)]2 (75560-03-1) + silver perchlorate → [PdClO4(C5H4N)(P(C6H5)3)]2 (90752-08-2)

Guidance literature:

In methanol; dichloromethane; byproducts: silver bromide; soln. of AgClO4 in MeOH added to CH2Cl2 soln. of Pd complex, stirred atroom temp. for 2 h; ppt. of AgBr filtered off, filtrate treated with deionized water, CH2Cl2 soln. passed through column of anhyd. Na2SO4, concd. under vac., Et2O added, ppt. filtered, washed with ether, dried in vac., purified by re-pptn. from CH2Cl2-Et2O; elem. anal.;

DOI:10.1246/bcsj.57.456

Reference yield: 85.2%

[PdClO4(C5H4N)(P(C6H5)3)]2 (90752-08-2) + potassium acetylacetonate (19393-11-4) → [Pd(CH3COCHCOCH3)(C5H4N)(P(C6H5)3)]

Guidance literature:

In methanol; dichloromethane; byproducts: potassium perchlorate; to soln. of Pd complex in CH2Cl2 added MeOH soln. of K(acac), stirred at room temp. for 20 min; filtered, evapd. in vac., CH2Cl2 added, filtered, concd. in vac., crystd. by addn. of Et2O, product filtered, washed with Et2O, recrystd. from CH2Cl2-Et2O; elem. anal.;

DOI:10.1246/bcsj.57.456

Reference yield: 46.9%

1,1,1-trifluoro-2,4-pentanedione potassium salt + [PdClO4(C5H4N)(P(C6H5)3)]2 (90752-08-2) → [Pd(CF3COCHCOCH3)(C5H4N)(P(C6H5)3)]

Guidance literature:

In methanol; dichloromethane; byproducts: potassium perchlorate; to soln. of Pd complex in CH2Cl2 added MeOH soln. of K(CF3COCHCOCH3), stirred at room temp. for 20 min; filtered, evapd. in vac., CH2Cl2 added, filtered, concd. in vac., crystd. by addn. of Et2O, product filtered, washed with Et2O, recrystd. from CH2Cl2-petroleum ether; elem. anal.;

DOI:10.1246/bcsj.57.456

upstream raw materials:

[PdBr(C₅H₄N)(P(C₆H₅)3)]2

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 90752-08-2 [PdClO₄(C₅H₄N)(P(C₆H₅)3)]2

Send

Send

Metric Ton KG G Pound L ML

Send

Send