[(CH₃)2C₃HN₂Al(((CH₃)2CH)2C₆H₃)2]B(C₆F₅)3

Base Information

• Chemical Name: [(CH₃)2C₃HN₂Al(((CH₃)2CH)2C₆H₃)2]B(C₆F₅)3
• CAS No.: 873297-05-3
• Molecular Formula: C₄₇H₄₁AlBF₁₅N₂
• Molecular Weight: 956.625
• Mol file: 873297-05-3.mol

Synonyms:

Chemical Property of [(CH₃)2C₃HN₂Al(((CH₃)2CH)2C₆H₃)2]B(C₆F₅)3

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [(CH₃)2C₃HN₂Al(((CH₃)2CH)2C₆H₃)2]B(C₆F₅)3

There total 1 articles about [(CH₃)2C₃HN₂Al(((CH₃)2CH)2C₆H₃)2]B(C₆F₅)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

(2,4-bis(2,6-diisopropylphenylimino)pentan-3-ide-.kappa2N,N')aluminum(I) (325465-25-6) + tris(pentafluorophenyl)borate (1109-15-5) → [(CH3)2C3HN2Al(((CH3)2CH)2C6H3)2]B(C6F5)3 (873297-05-3)

Guidance literature:

In toluene; N2 or Ar, Schlenk and glove-box techniques; toluene added to a mixture of Al-compd. and B-compd. at -78°C, stirred, slowly warmed to roomtemp., sirred for 15 h; solv. removed in vac., hexane added, filtered, stored for two weeks at room temp., elem. anal.;

DOI:10.1002/anie.200502251

upstream raw materials:

(2,4-bis(2,6-diisopropylphenylimino)pentan-3-ide-.kappa2N,N')aluminum(I)

tris(pentafluorophenyl)borate