(C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br

Base Information

Chemical Name:(C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br
CAS No.:914931-30-9
Molecular Formula:C₄₀H₄₁BrFeP₂
Molecular Weight:719.464
Hs Code.:

(C<sub>5</sub>(CH<sub>3</sub>)5)Fe(P(C<sub>6</sub>H<sub>5</sub>)2C<sub>2</sub>H<sub>4</sub>P(C<sub>6</sub>H<sub>5</sub>)2)C<sub>2</sub>C<sub>2</sub>H<sub>2</sub>Br

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Chemical Property of (C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br

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Technology Process of (C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br

There total 1 articles about (C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 540-49-8
cis+trans-dibromoethylene

: (η(2)-1,2-bis(diphenylphosphino)ethane)(η(5)-pentamethylcyclopentadienyl)Fe-C.tplbond.CH

: 915040-07-2,914931-30-9
(C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br

Guidance literature:: With triethylamine; catalyst:[PdCl₂(P(C₆H₅)3)2]/CuI; In tetrahydrofuran; (Schlenk, inert atm.) to a mixt. of complexes, CuI and ethene-compound were added degassed N(C2H5)3 and THF, the mixt. was stirred for 40 h at room temp.; volatiles were removed under reduced pressure, the residue was extd. with ether, passed through an alumina pad, evapd., extd. with pentane, the oil was triturated with pentane at -78°C;
DOI:10.1021/om060403t

Reference yield:

: (η(2)-1,2-bis(diphenylphosphino)ethane)(η(5)-pentamethylcyclopentadienyl)Fe-C.tplbond.CH

: 915040-07-2,914931-30-9
(C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2)C₂C₂H₂Br

: [(η5-C5Me5)(η2-1,2-bis(diphenylphosphino)ethane)Fe-C2-C2-Fe(η2-1,2-bis(diphenylphosphino)ethane)(η5-C5Me5)]

: 914931-31-0
((C₅(CH₃)5)Fe(P(C₆H₅)2C₂H₄P(C₆H₅)2))C₂CHCH₂

Guidance literature:: With catalyst:[PdCl₂(P(C₆H₅)3)2]/CuI; In triethylamine; (Schlenk, inert atm.) the mixt. of complexes and CuI in N(C2H5)3 for 45 h at room temp.; volatiles were removed under reduced pressure, the residue was extd. with ether, passed through an alumina pad, evapd., extd. with pentane, the oil was triturated with pentane at -78°C;
DOI:10.1021/om060403t