C₃₄H₃₀NO₄⁽¹⁺⁾*Cl^(1-)

Base Information

• Chemical Name: C₃₄H₃₀NO₄⁽¹⁺⁾*Cl^(1-)
• CAS No.: 1235871-09-6
• Molecular Formula: C₃₄H₃₀NO₄*Cl
• Molecular Weight: 552.07
• Mol file: 1235871-09-6.mol

Synonyms:

Chemical Property of C₃₄H₃₀NO₄⁽¹⁺⁾*Cl^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₃₀NO₄⁽¹⁺⁾*Cl^(1-)

There total 7 articles about C₃₄H₃₀NO₄⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C34H30BrNO5 (1235871-50-7) → C34H30NO4(1+)*Cl(1-) (1235871-09-6)

Guidance literature:

C₃₄H₃₀BrNO₅; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃;

With hydrogenchloride; In water;

DOI:10.1016/j.bmcl.2012.09.097

Reference yield:

C33H28BrNO5 (1235871-49-4) → C34H30NO4(1+)*Cl(1-) (1235871-09-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.09.097

Reference yield:

6-bromo-2,3-dimethoxybenzoic acid (60555-93-3) → C34H30NO4(1+)*Cl(1-) (1235871-09-6)

Guidance literature:

Multi-step reaction with 4 steps

1: oxalyl dichloride / dichloromethane / 45 °C

2: triethylamine / dichloromethane / 20 °C

3: sodium hydride / N,N-dimethyl-formamide / 20 °C

4: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

With lithium aluminium tetrahydride; oxalyl dichloride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1016/j.bmcl.2012.09.097

upstream raw materials:

C₃₃H₂₈BrNO₅

6-bromo-2,3-dimethoxybenzoic acid

1-bromo-5-nitro-2,3-dimethoxynaphthalene

1-(biphenyl[1,1']-4-yl)-2,3-dimethoxy-5-nitronaphthalene