3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride

Base Information

Chemical Name:3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride
CAS No.:81653-63-6
Molecular Formula:C₂₀H₃₁NO₆*ClH
Molecular Weight:417.93
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride

Chemical Property:

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Technology Process of 3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride

There total 3 articles about 3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18997-19-8
Chloromethyl pivalate

: 81653-63-6
3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / NaI / acetone / 5 h / Ambient temperature

2: 88 percent / K₂CO₃ / acetone / 6 h / Ambient temperature

3: 90 percent / anhyd. HCl / ethyl acetate / 0.17 h / 0 °C

With hydrogenchloride; potassium carbonate; sodium iodide; In ethyl acetate; acetone;
DOI:10.1021/jo00174a024

Reference yield:

: 645-31-8
3-hydroxytyramine hydrobromide

: 81653-63-6
3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / 70percent aqu. triethylamine / dioxane / 5 h / Ambient temperature

2: 88 percent / K₂CO₃ / acetone / 6 h / Ambient temperature

3: 90 percent / anhyd. HCl / ethyl acetate / 0.17 h / 0 °C

With hydrogenchloride; potassium carbonate; triethylamine; In 1,4-dioxane; ethyl acetate; acetone;
DOI:10.1021/jo00174a024

Reference yield:

: 37034-31-4
N-(tert-butoxycarbonyl)dopamine

: 81653-63-6
3,4-bis<(pivalyloxy)methyl>dopamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / K₂CO₃ / acetone / 6 h / Ambient temperature

2: 90 percent / anhyd. HCl / ethyl acetate / 0.17 h / 0 °C

With hydrogenchloride; potassium carbonate; In ethyl acetate; acetone;
DOI:10.1021/jo00174a024