3-Amino-N-(4-bromophenyl)propanamide hydrochloride

Base Information

• Chemical Name: 3-Amino-N-(4-bromophenyl)propanamide hydrochloride
• CAS No.: 1193388-90-7
• Molecular Formula: C₉H₁₁BrN₂O*ClH
• Molecular Weight: 279.564
• Mol file: 1193388-90-7.mol

Synonyms:

Chemical Property of 3-Amino-N-(4-bromophenyl)propanamide hydrochloride

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3-Amino-N-(4-bromophenyl)propanamideHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-Amino-N-(4-bromophenyl)propanamide hydrochloride

There total 2 articles about 3-Amino-N-(4-bromophenyl)propanamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tert-butyl (3-((4-bromophenyl)amino)-3-oxopropyl)carbamate → 3-amino-N-(4-bromophenyl)propanamide hydrochloride salt (1193388-90-7)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃;

DOI:10.1016/j.chembiol.2019.09.004

Reference yield:

4-bromo-aniline (106-40-1) → 3-amino-N-(4-bromophenyl)propanamide hydrochloride salt (1193388-90-7)

Guidance literature:

Multi-step reaction with 2 steps

1: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

2: hydrogenchloride / 1,4-dioxane; water / 20 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In 1,4-dioxane; dichloromethane; water;

DOI:10.1016/j.chembiol.2019.09.004

upstream raw materials:

4-bromo-aniline

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