pentachlorobenzyl mercuric bromide

Base Information

• Chemical Name: pentachlorobenzyl mercuric bromide
• CAS No.: 97578-10-4
• Molecular Formula: C₇H₂BrCl₅Hg
• Molecular Weight: 543.852
• Mol file: 97578-10-4.mol

Synonyms:

Chemical Property of pentachlorobenzyl mercuric bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of pentachlorobenzyl mercuric bromide

There total 2 articles about pentachlorobenzyl mercuric bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

α-bromo-2,3,4,5,6-pentachlorotoluene (36593-26-7) + mercury → pentachlorobenzyl mercuric bromide (97578-10-4)

Guidance literature:

With catalyst: Et₄NBr; In N,N-dimethyl-formamide; byproducts: (C6Cl5CH2)2; mixt. of pentachlorobenzyl bromide and Hg in satd. soln. of Et4NBr in dry DMF agitated (sealed ampoule, in the dark, 170 h);; ppt. filtered off, washed with ether, dried, (chromy. of the mother liquor: silica gel, CHCl3-hexane, protected from light); elem. anal.;;

DOI:10.1007/BF00947734

Reference yield:

α-bromo-2,3,4,5,6-pentachlorotoluene (36593-26-7) + mercury → pentachlorobenzyl mercuric bromide (97578-10-4) + decachlorodibenzyl

Guidance literature:

In chloroform; Irradiation (UV/VIS); mixt. of pentachlorobenzyl bromide and Hg in CHCl3 agitated (sealed ampoule, UV irradn., 60 h);;

DOI:10.1007/BF00947734

upstream raw materials:

α-bromo-2,3,4,5,6-pentachlorotoluene