α-bromo-2,3,4,5,6-pentachlorotoluene

Base Information

Chemical Name:α-bromo-2,3,4,5,6-pentachlorotoluene
CAS No.:36593-26-7
Molecular Formula:C₇H₂BrCl₅
Molecular Weight:343.262
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of α-bromo-2,3,4,5,6-pentachlorotoluene

Chemical Property:

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Technology Process of α-bromo-2,3,4,5,6-pentachlorotoluene

There total 2 articles about α-bromo-2,3,4,5,6-pentachlorotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 877-11-2
pentachlorotoluene

: 36593-26-7
α-bromo-2,3,4,5,6-pentachlorotoluene

Guidance literature:: With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; Heating;
DOI:10.1016/S0022-328X(00)89735-1

Reference yield:

: 36593-26-7
α-bromo-2,3,4,5,6-pentachlorotoluene

Guidance literature:: Pentachlortoluol, 1)SO3 2)CBr4/C2Cl4;

Reference yield: 66.0%

: 36593-26-7
α-bromo-2,3,4,5,6-pentachlorotoluene

: mercury

: 97578-10-4
pentachlorobenzyl mercuric bromide

Guidance literature:: With catalyst: Et₄NBr; In N,N-dimethyl-formamide; byproducts: (C6Cl5CH2)2; mixt. of pentachlorobenzyl bromide and Hg in satd. soln. of Et4NBr in dry DMF agitated (sealed ampoule, in the dark, 170 h);; ppt. filtered off, washed with ether, dried, (chromy. of the mother liquor: silica gel, CHCl3-hexane, protected from light); elem. anal.;;
DOI:10.1007/BF00947734