α-bromo-2,3,4,5,6-pentachlorotoluene

Base Information

• Chemical Name: α-bromo-2,3,4,5,6-pentachlorotoluene
• CAS No.: 36593-26-7
• Molecular Formula: C₇H₂BrCl₅
• Molecular Weight: 343.262
• Mol file: 36593-26-7.mol

Synonyms:

Chemical Property of α-bromo-2,3,4,5,6-pentachlorotoluene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-bromo-2,3,4,5,6-pentachlorotoluene

There total 2 articles about α-bromo-2,3,4,5,6-pentachlorotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pentachlorotoluene (877-11-2) → α-bromo-2,3,4,5,6-pentachlorotoluene (36593-26-7)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In tetrachloromethane; Heating;

DOI:10.1016/S0022-328X(00)89735-1

Reference yield:

→ α-bromo-2,3,4,5,6-pentachlorotoluene (36593-26-7)

Guidance literature:

Pentachlortoluol, 1)SO3 2)CBr4/C2Cl4;

Reference yield: 66.0%

α-bromo-2,3,4,5,6-pentachlorotoluene (36593-26-7) + mercury → pentachlorobenzyl mercuric bromide (97578-10-4)

Guidance literature:

With catalyst: Et₄NBr; In N,N-dimethyl-formamide; byproducts: (C6Cl5CH2)2; mixt. of pentachlorobenzyl bromide and Hg in satd. soln. of Et4NBr in dry DMF agitated (sealed ampoule, in the dark, 170 h);; ppt. filtered off, washed with ether, dried, (chromy. of the mother liquor: silica gel, CHCl3-hexane, protected from light); elem. anal.;;

DOI:10.1007/BF00947734

upstream raw materials:

pentachlorotoluene

Downstream raw materials:

Pentachlor-benzylnitrat

1-bromo-2,3,4,5,6-pentachlorobenzene

2,3,4,5,6-Pentachlor-benzylamin

acetic acid-(2,3,4,5,6-pentachloro-benzyl ester)