Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-2-(2,3,4-trimethoxyphenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester

Base Information

Chemical Name:Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-2-(2,3,4-trimethoxyphenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester
CAS No.:135696-27-4
Molecular Formula:C19H24N6O8
Molecular Weight:464.435
Hs Code.:
Mol file:135696-27-4.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-2-(2,3,4-trimethoxyphenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-2-(2,3,4-trimethoxyphenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester

There total 2 articles about Carbamic acid, [6-amino-4-[[2-(hydroxyimino)-2-(2,3,4-trimethoxyphenyl)ethyl]amino]-5- nitro-2-pyridinyl]-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 135696-15-0
2-Amino-1-(2,3,4-trimethoxy-phenyl)-ethanone oxime

: 6506-86-1
ethyl (6-amino-4-chloro-5-nitropyridin-2-yl)carbamate

: 135696-27-4
{6-Amino-4-[2-[(E)-hydroxyimino]-2-(2,3,4-trimethoxy-phenyl)-ethylamino]-5-nitro-pyridin-2-yl}-carbamic acid ethyl ester

Guidance literature:: With triethylamine; In ethanol; for 1.5h; Heating;
DOI:10.1021/jm00115a005

Reference yield:

: 135696-60-5
2-[2-[(E)-Hydroxyimino]-2-(2,3,4-trimethoxy-phenyl)-ethyl]-isoindole-1,3-dione

: 135696-27-4
{6-Amino-4-[2-[(E)-hydroxyimino]-2-(2,3,4-trimethoxy-phenyl)-ethylamino]-5-nitro-pyridin-2-yl}-carbamic acid ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 21 h / 40 °C

2: 50 percent / triethylamine / ethanol / 1.5 h / Heating

With triethylamine; hydrazine; In ethanol;
DOI:10.1021/jm00115a005